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The Effect of the Infrared Laser Pre-heating on Ultraviolet Picosecond Laser Polishing of SiC Ceramics

Received: 25 March 2025     Accepted: 18 May 2025     Published: 11 June 2025
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Abstract

The ultraviolet laser has been used to polish SiC ceramics by its thermal and photochemical effect in previous works to resolve the application limitation of the SiC ceramics for the demand of high-precision applications. In this paper, the "cold polishing" technology of SiC ceramics under photon absorption was studied by using the 355nm ultraviolet picosecond laser, the surface roughness was reduced from Ra=1.616μm to Ra=1.087μm only even though the polishing process parameters has been optimized, because the thermal effect such as gasification was found due to the ablation threshold, and the surface quality of brittle ceramics might be degraded by thermal effect during laser polishing. The ablation threshold of the SiC was obtained as about 0.3J/cm2. The method of ultraviolet picosecond laser "cold polishing" with infrared laser as preheating source was innovatively proposed to promote the photon-absorption process. By adjusting the preheating process parameters of the infrared laser, the macroscopic morphology and microstructure of polished SiC ceramic surface were analyzed, so as to further clarify the mechanism of photon-absorption effect during the polishing process. It was found that the “cold polishing” by the photon absorption can be promoted owing to the decrease of the ablation threshold under the infrared laser preheating process. Defects such as cracks and porosity cannot be found under the 200× optical microscope, the surface roughness of about 0.66μm can be obtained compared with the 1.087μm by the polishing of ultraviolet picosecond laser. Thus, the ultraviolet picosecond laser polishing with infrared laser preheating technology can be used as the high precise and high efficient polishing technology for the SiC ceramics.

Published in American Journal of Environmental Science and Engineering (Volume 9, Issue 2)
DOI 10.11648/j.ajese.20250902.14
Page(s) 68-75
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This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.

Copyright

Copyright © The Author(s), 2025. Published by Science Publishing Group

Keywords

SiC Ceramics, Ultraviolet Picosecond Laser, Photon Absorption, Ablation Threshold, Cold Polishing

1. Introduction
Due to the excellent thermal resistance and mechanical properties, silicon carbide ceramic materials are widely used in electronic devices, aerospace, semiconductor industry, and biomedicine . However, due to the poor surface quality of ceramic devices caused by the traditional manufacturing process, the applications of ceramic devices in high precision environment are severely limited. The polishing of ceramic parts has always been the bottleneck of modern manufacturing industry. Chemical, mechanical or electrochemical polishing methods are always adopted in the traditional ceramic polishing process , which have a series of problems such as poor machining accuracy, low efficiency, serious pollution, and lack of consistency and stability of product quality. Due to the incompatibility of the requirements of modern manufacturing equipment to achieve high automation, intelligence and network, it is very important to choose or develop a new ceramic polishing process.
In recent years, laser processing technology has developed rapidly, ranging from laser cutting and welding in the field of large-scale processing to fine and deep hole processing and microstructural functional surface manufacturing in the field of micro-processing, the application of laser processing technology has been increasingly extensive . Compared with a variety of traditional polishing processes, laser polishing is a contactless processing method with no pollution, high efficiency, high processing flexibility and consistency, and is a new laser processing application technology .
Recently, massive research work has been done on the polishing of metal materials in the domestic and overseas, and high surface quality of the metal piece such can be achieved by laser polishing. Not only the surface roughness and the residual stress and of metal parts could be greatly reduced, but also surface hardness, wear resistance and fatigue strength and of metal parts could be strengthened by the laser polishing process. The laser polishing of metal pieces are mainly divided into continuous-laser polishing and pulsed-laser polishing. The continuous laser is mainly used for rough polishing, while pulsed laser is mainly used for fine polishing . The research on laser polishing of 3D printed parts has been carried out in Beihang Univeristy . Xiao et al. recently conducted a study on laser polishing assisted by steady-state magnetic field, and the roughnesse of the steel piece (Ra=1.87μm) was reduces to Ra=0.18μm by a large scale. Temmler et al. studied the polishing of stainless steel by pulsed laser, and the roughness of the polished surface was reduced by 92%.
Compared with the metal material, few researches on laser polishing of ceramic parts could be found due to the high melting point, high hardness, high viscosity and greater brittleness of ceramic materials . In the process of ceramic polishing based on short pulse laser, the melting, gasification, microcrack and photochemical interaction of ceramic materials could be found. Therefore, it is urgent to study the mechanism of laser polishing ceramics, so as to achieve high precision polishing of ceramic parts. The polishing process for the brittle ceramic parts are mainly divided into thermal polishing and photochemical polishing principle, according to different laser polishing mechanism. For IR laser, the polishing process is mainly conducted by thermal effect of laser. And for UV laser, the polishing process is mainly conducted by the photochemical effect of laser . The thermal polishing process means that the working piece absorbing laser energy to achieve melting flow, gasification removal or thermal stress removal. Laser photochemical polishing means that after laser irradiation on the surface of the material, the material directly absorbs photon energy to break the chemical bond of the material or destroy the structure of the lattice, so as to achieve the removal of the material.
The current research on laser polishing ceramics at home and abroad mainly focuses on the thermal effect in the process . The reduction of the surface roughness was mainly by the grain growth and "melting peak filling" of polishing molten pool. Li Weibo obtained smaller surface roughness under optimized process parameters during the polishing of SiC ceramics with 800nm femtosecond laser . The roughness of 2.5μm was realized by 30W Yb: YAG laser polishing of alumina ceramics . The polishing process was mainly based on the thermal effects such as the melting of the ceramic pieces. Ji et al. reduced the surface roughness of ZrO2 ceramics to 2.84μm by 6ns pulsed laser, and the polishing process was mainly through the melting and evaporation of the materials. Zhang et al. carried out the polishing of alumina ceramics by 1064nm picosecond pulse laser, and by controlling the laser polishing process, the ceramic surface was recrystallized, and the surface roughness of ceramic could be reduced from 1.8μm to 0.32μm .
Owing to the brittleness of SiC ceramics, the heat stress during the polishing process by thermal effect of the laser would lead to the cracks of the ceramic pieces. The thermal stress was small in the process of laser polishing by photochemistry effect, and almost no cracks would be found after processing, which was especially suitable for high precision polishing of brittle ceramics. In recent years, some progress has been made in the polishing of alumina ceramics by 355nm UV laser has also made . In terms of material surface removal, LIU et al. proposed multi-photon absorption effect to explain the energy absorption caused by the femtosecond laser processing on dielectric materials. Zhao Qingliang et al. used femtosecond laser micromachining system to conduct theoretical and experimental research on the ablation characteristics of SiC ceramics, and analyzed the multi-photon absorption during laser processing of SiC ceramics.
Since the band gap energy of SiC ceramics is about 3eV, the infrared laser with low photon energy is easy to cause the thermal effect during the polishing process through multi-photon absorption. The single-photon energy for 355nm UV laser is higher, so it has more advantages in removing ceramic surface roughness by photochemistry effect. In order to further analyze the mechanism of UV laser polishing ceramics, so as to further reduce the thermal stress in the polishing process. This paper innovatively proposed the method of ultraviolet picosecond laser "cold polishing" with infrared laser as preheating source to promote the photon-absorption process. The roughness removal mechanisms and surface morphology by different process parameters during the ceramic polishing was studied, thus greatly optimize the ceramic surface quality and provide technical basis for realizing high efficiency and high precision polishing of SiC ceramics.
2. Experiment
2.1. Preparation and Characterization of Liners and Fillers
The SiC ceramic used in this paper with the characteristics of high wear resistance and high hardness belonged to high temperature resistant structural materials. The EDS of the cermic samples was shown in Figure 1, and its chemical composition is shown in Table 1. It can be seen from Table 1 that the SiC ceramic maintained high purity in the preparation process. The samples were cut into 50mm*50mm*10mm ceramic plates CNC scribing cutting machine. Before laser polishing, the plate washing water was used for cleaning, as shown in Figure 2. The original roughness of the samples measured by white light interferometer was 1.616μm.
Figure 1. EDS of the SiC ceramics.
Table 1. Chemical composition of SiC ceramic samples.

Map Sum Spectrum

Element

Wt%

Wt% Sigma

Atomic %

C

36.6

0.33

57.16

O

0.98

0.08

1.15

Si

62.41

0.33

41.68

Total:

100

100

Figure 2. Original surface morphology and roughness of samples.
2.2. Laser Polishing Procedure
The 355nm UV picosecond laser polishing system is shown in 3, including 30W UV picosecond pulse laser, scanning galvanometer, beam shaping output mirror, five-axis CNC system, processing table, water cooling system, etc. The focal length of the UV laser is 170mm, as shown in Figure 4. The beam spot of the UV laser is a Gaussian spot with a diameter of about 1.8mm, and the beam diameter after the output focusing lens is about 40μm. The laser polishing process of SiC ceramic is shown in Figure 5. The single polishing area of SiC ceramic was adjusted to 5mm*5mm by scanning galvanometer. The power percentage of the UV laser was 20%-50% with the span of 10%. The scanning path spacing was 0.001-0.007mm with the span of 0.002mm. The scanning speed of the UV laser was 1200-1600mm/s with the span of 100mm/s. Orthogonal test was carried out by adjusting laser process parameters. At the same time, the effect of 800nm infrared continuous laser preheating on UV laser polishing of SiC ceramics was studied (as shown in Figure 6), and the mechanism of the surface roughness reduction due to photon absorption effect during SiC ceramic polishing was further analyzed.
The white light interferometer (BRUKER WYKO Contour GT-K) was used to directly measure the surface roughness of continuous laser polishing, and the 3D microstructure was obtained. The defects of the polished surface were further analyzed by optical microscopy. The microstructure and the metallographic of the polished workpiece was determined by ZEISS SIGMA 500/VP and GeminiSEM 300.
Figure 3. UV picosecond laser polishing system.
Figure 4. Beam spot of the UV laser.
Figure 5. Schematic diagram of the UV laser polishing process.
Figure 6. Schematic diagram of the UV laser polishing process under the preheating of IR laser.
3. Result and Discussion
3.1. Effect of Different Polishing Process on Surface Roughness by UV Laser
Figure 7 represents the surface of the pieces under different polishing processes with scanning speed of 1600mm/s. Roughness detection of polished samples under different UV picosecond laser parameters shows that the roughness Ra of SiC sample surface decreases first and then increases with the increase of laser power when the scanning spacing is unchanged, as shown in Figure 8. Figures 8 (a)-(d) represent the surface roughness of the polished sample with the scanning spacing of 0.003mm and the power percentage of 20%-50%.
Figure 7. Surface morphology of samples under different laser polishing processes.
Figure 8. Surface roughness of SiC under different laser power: (a) 20%; (b) 30%; (c) 40%; (d) 50%.
Thermal phenomena such as material volatilization and surface destruction of brittle SiC ceramics appear at the beginning of the polishing process. And there was no "hot polishing" defects such as cracks, porosity in the microstructure of the polished ceramic samples detected by 200X optical microscope under different laser power (Figure 9). It shows that in the process of UV picosecond laser polishing, the cold polishing process of photon absorption was still the main process, but there was still the influence of laser thermal effect during the polishing process. The band gap energy of SiC ceramics is 3eV, and the single photon energy of 355nm UV picosecond laser is about 3.5eV, which meets photon absorption of the SiC ceramics. However, the thermal evaporation of the samples existed in the polishing process, which indicated that the thermal effect existed in the polishing process. This phenomenon is consistent with the results of previous studies . Therefore, when the power percentage was 20%, the laser heat accumulation process was accompanied by the ablation of the sample surface. When the power is gradually increased, it was easier to reach the threshold of multiphoton absorption effect, and the "cold polishing" effect was gradually obvious, and the roughness would be further reduced. When the laser power was too high, excess heat accumulation at the initial stage of polishing, which would lead to the melting and redeposition on the sample surface, and thus reducing the surface roughness. Figure 10 shows the 3D topography of the polished sample. It can be seen from Figure 10 that when the laser power increased from 20% to 30%, the surface roughness would be reduced due to the obvious "cold polishing" effect. However, when the laser power further increased, the ablation effect of heat accumulation would form volatile deposition on the sample and increase the surface roughness.
Figure 9. Surface morphology of SiC ceramic under different laser power: (a) 20%; (b) 30%; (c) 40%; (d) 50%.
Figure 10. 3D morphology of SiC ceramic surface under different laser power: (a) 20%; (b) 30%; (c) 40%; (d) 50%.
As shown in Figure 11, when the laser scanning speed was 1600mm/s and the laser power percentage was 20%, the roughness of the polished sample decreased first and then increased with the increase of the scanning speed. This experimental phenomenon can also be explained by the "cold polishing" threshold of photon absorption. When the laser scanning paths overlap, the previous laser polishing process would preheat the next polishing process, and the laser polishing process could achieve the "cold polishing" process of photon absorption faster, so as to achieve the reduction of surface roughness. Because the IR laser used in the experiment was a Gaussian beam, the preheating effect was obviously weakened when the laser scanning paths overlap less, and the thermal effect during the polishing process was more obvious, and the polishing quality of SiC ceramic with high temperature resistance and viscosity was weakened. In particular, when the laser power was lower than 10% and the scanning distance was 0.001mm, the heat accumulation effect was more obvious, and the surface quality was extremely deteriorated with the roughness of 3.707μm. Therefore, it can be seen that in order to improve the surface quality of SiC ceramics, it is necessary to reduce the heat accumulation as much as possible before the threshold of cold action polishing was reached.
Figure 11. Surface roughness of SiC ceramics at different scan spacing: (a) 0.001mm; (b) 0.003mm; (c) 0.005mm; (d) 0.007%.
3.2. Effect of IR Laser Preheating on UV Laser Polishing of SiC Ceramics
Similarly, in the experimental process of UV laser polishing under IR laser preheating, the roughness can also be reduced to 0.66μm by adjusting the preheating process. Since there would be a good prospect in the field of semiconductor technology for SiC ceramics, the dual laser polishing of SiC ceramic substrates with the roughness about 0.16μm was also investigated. With the optimized UV laser parameters, it was found that the preheating process would improve the surface quality of SiC substrates. The roughness of about 0.025μm was achieved by the UV laser with the optimized parameters. Nevertheless, under the preheating of IR laser, the roughness of about 0.20μm was achieved.
4. Conclusion
(1) The orthogonal test results showed that when the laser power percentage was 30%, the scanning path spacing was 0.005mm, and the laser scanning speed was 1600mm/s, the surface roughness was further reduced from 1.616μm to 1.087μm. Compared with the traditional mechanical polishing process, the polishing efficiency was significantly increased by more than 3 times.
(2) The laser polishing process was accompanied by the "cold polishing" and "hot polishing" process. The experimental results showed that the polishing process of SiC ceramics by 355nm UV picosecond laser mainly exhibits two forms: material gasification and surface material removal after the photon absorption effect. By optimizing the laser polishing parameters, the "photon absorption" effect during polishing process can be realized faster, and the surface roughness of SiC ceramics can be effectively reduced by reducing the heat accumulation effect.
(3) The UV laser polishing of ceramic pieces under the preheating of IR laser was proposed. By adjusting and optimizing the infrared laser preheating parameters, the ceramics can be polished with high efficiency and high quality.
Acknowledgments
This work was supported by Science and Technology Project of Guangdong Province (grant no. 2021A0505030013), Shenzhen Science and Technology Plan (grant nos.KJDZ20231023100000001), and Shenzhen Institute of Information Technology Project (HX0565, HX0664).
Conflicts of Interest
The authors declare no conflicts of interest.
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    Luo, B., Xiao, H., Zhou, Y., Liu, M., Xu, X., et al. (2025). The Effect of the Infrared Laser Pre-heating on Ultraviolet Picosecond Laser Polishing of SiC Ceramics. American Journal of Environmental Science and Engineering, 9(2), 68-75. https://doi.org/10.11648/j.ajese.20250902.14

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    Luo, B.; Xiao, H.; Zhou, Y.; Liu, M.; Xu, X., et al. The Effect of the Infrared Laser Pre-heating on Ultraviolet Picosecond Laser Polishing of SiC Ceramics. Am. J. Environ. Sci. Eng. 2025, 9(2), 68-75. doi: 10.11648/j.ajese.20250902.14

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    AMA Style

    Luo B, Xiao H, Zhou Y, Liu M, Xu X, et al. The Effect of the Infrared Laser Pre-heating on Ultraviolet Picosecond Laser Polishing of SiC Ceramics. Am J Environ Sci Eng. 2025;9(2):68-75. doi: 10.11648/j.ajese.20250902.14

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  • @article{10.11648/j.ajese.20250902.14,
      author = {Bowei Luo and Haibing Xiao and Yongquan Zhou and Mingjun Liu and Xiaomei Xu and Wei Zhang},
      title = {The Effect of the Infrared Laser Pre-heating on Ultraviolet Picosecond Laser Polishing of SiC Ceramics
    },
      journal = {American Journal of Environmental Science and Engineering},
      volume = {9},
      number = {2},
      pages = {68-75},
      doi = {10.11648/j.ajese.20250902.14},
      url = {https://doi.org/10.11648/j.ajese.20250902.14},
      eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ajese.20250902.14},
      abstract = {The ultraviolet laser has been used to polish SiC ceramics by its thermal and photochemical effect in previous works to resolve the application limitation of the SiC ceramics for the demand of high-precision applications. In this paper, the "cold polishing" technology of SiC ceramics under photon absorption was studied by using the 355nm ultraviolet picosecond laser, the surface roughness was reduced from Ra=1.616μm to Ra=1.087μm only even though the polishing process parameters has been optimized, because the thermal effect such as gasification was found due to the ablation threshold, and the surface quality of brittle ceramics might be degraded by thermal effect during laser polishing. The ablation threshold of the SiC was obtained as about 0.3J/cm2. The method of ultraviolet picosecond laser "cold polishing" with infrared laser as preheating source was innovatively proposed to promote the photon-absorption process. By adjusting the preheating process parameters of the infrared laser, the macroscopic morphology and microstructure of polished SiC ceramic surface were analyzed, so as to further clarify the mechanism of photon-absorption effect during the polishing process. It was found that the “cold polishing” by the photon absorption can be promoted owing to the decrease of the ablation threshold under the infrared laser preheating process. Defects such as cracks and porosity cannot be found under the 200× optical microscope, the surface roughness of about 0.66μm can be obtained compared with the 1.087μm by the polishing of ultraviolet picosecond laser. Thus, the ultraviolet picosecond laser polishing with infrared laser preheating technology can be used as the high precise and high efficient polishing technology for the SiC ceramics.
    },
     year = {2025}
    }
    

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  • TY  - JOUR
    T1  - The Effect of the Infrared Laser Pre-heating on Ultraviolet Picosecond Laser Polishing of SiC Ceramics
    
    AU  - Bowei Luo
    AU  - Haibing Xiao
    AU  - Yongquan Zhou
    AU  - Mingjun Liu
    AU  - Xiaomei Xu
    AU  - Wei Zhang
    Y1  - 2025/06/11
    PY  - 2025
    N1  - https://doi.org/10.11648/j.ajese.20250902.14
    DO  - 10.11648/j.ajese.20250902.14
    T2  - American Journal of Environmental Science and Engineering
    JF  - American Journal of Environmental Science and Engineering
    JO  - American Journal of Environmental Science and Engineering
    SP  - 68
    EP  - 75
    PB  - Science Publishing Group
    SN  - 2578-7993
    UR  - https://doi.org/10.11648/j.ajese.20250902.14
    AB  - The ultraviolet laser has been used to polish SiC ceramics by its thermal and photochemical effect in previous works to resolve the application limitation of the SiC ceramics for the demand of high-precision applications. In this paper, the "cold polishing" technology of SiC ceramics under photon absorption was studied by using the 355nm ultraviolet picosecond laser, the surface roughness was reduced from Ra=1.616μm to Ra=1.087μm only even though the polishing process parameters has been optimized, because the thermal effect such as gasification was found due to the ablation threshold, and the surface quality of brittle ceramics might be degraded by thermal effect during laser polishing. The ablation threshold of the SiC was obtained as about 0.3J/cm2. The method of ultraviolet picosecond laser "cold polishing" with infrared laser as preheating source was innovatively proposed to promote the photon-absorption process. By adjusting the preheating process parameters of the infrared laser, the macroscopic morphology and microstructure of polished SiC ceramic surface were analyzed, so as to further clarify the mechanism of photon-absorption effect during the polishing process. It was found that the “cold polishing” by the photon absorption can be promoted owing to the decrease of the ablation threshold under the infrared laser preheating process. Defects such as cracks and porosity cannot be found under the 200× optical microscope, the surface roughness of about 0.66μm can be obtained compared with the 1.087μm by the polishing of ultraviolet picosecond laser. Thus, the ultraviolet picosecond laser polishing with infrared laser preheating technology can be used as the high precise and high efficient polishing technology for the SiC ceramics.
    
    VL  - 9
    IS  - 2
    ER  - 

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Author Information
  • School of Intelligent Manufacturing and Equipment, Shenzhen Institute of Information Technology, Shenzhen, China

  • School of Intelligent Manufacturing and Equipment, Shenzhen Institute of Information Technology, Shenzhen, China

  • School of Intelligent Manufacturing and Equipment, Shenzhen Institute of Information Technology, Shenzhen, China

  • School of Intelligent Manufacturing and Equipment, Shenzhen Institute of Information Technology, Shenzhen, China

  • School of Intelligent Manufacturing and Equipment, Shenzhen Institute of Information Technology, Shenzhen, China

  • School of Intelligent Manufacturing and Equipment, Shenzhen Institute of Information Technology, Shenzhen, China